The SPME-LC fiber probes are intended as single-use devices for the extraction of small molecules out of a fluid followed by solvent desorption and LC analysis.Traditional solid phase microextraction (SPME) fibers were developed with common GC type phases, which were primarily designed for extraction of volatile or semi-volatile compounds using thermal desorption as the means of introducing sample into the chromatographic colu…
Carboxen®/Polydimethylsiloxane (CAR/PDMS) SPME FibersSolid Phase Microextraction (SPME) is an innovative, solvent-free sample prep technology that is fast, economical, and versatile. SPME uses a fiber coated with a liquid (polymer), a solid (sorbent), or a combination of both. The fiber coating removes the compounds from your sample by absorption in the case of liquid coatings or adsorbtion in the case of solid coatings. The…
Divinylbenzene/Carboxen/Polydimethylsiloxane (DVB/CAR/PDMS) SPME FibersSolid Phase Microextraction (SPME) is an innovative, solvent-free sample prep technology that is fast, economical, and versatile. SPME uses a fiber coated with a liquid (polymer), a solid (sorbent), or a combination of both. The fiber coating removes the compounds from your sample by absorption in the case of liquid coatings or adsorbtion in the case of sol…
The Perfect Combination of Low Bleed, Thermal Stability, and Easy Puncturability!Molded Thermogreen LB-2 septa are manufactured from high quality, low bleed material using the same exclusive LB-2 rubber formulation that chromatographers are accustomed to using. The difference is that molded septa, unlike traditional die-cut septa, offer easier installation and better sealing inside the injection port. This is because our liqui…
Supelco provides high quality derivatization reagents for silylation.Silylation is the most widely used derivatization technique. Functional groups that present a problem with gas chromatogaphy detection - hydroxyl, carboxylic acid, amine, thiol, phosphate - can be derivatized by silylation reagents. Silylation involves replacement of the acidic hydrogen with an alkylsilyl group, for example, -SiMe3.Silylation derivatives are…
Supelco provides high quality derivatization reagents for acylation.Acylation, an alternative to silylation, allows the conversion of compounds with active hydrogen such as -OH, -SH, and -NH into esters, thioesters and amines, respectively. A very popular example of this method is the insertion of perfluoracyl groups to enable electron capture detection (ECD). Carbonyl groups adjacent to halogenated carbons enhance the ECD res…
Supelco provides high quality derivatization reagents for akylation and esterification.Alkylation is the replacement of the active hydrogen in R-COOH, R-OH, R-SH, R-NH, R-NH2, R-CONH2, R-CONH-R′ with an alkyl group, or sometimes an aryl group.Esterification is the first choice for derivatization of carboxylic acids and other acidic functional groups. Acids are reactive compounds, and are too polar to be well separated by gas c…
Supelco® has developed a line of high performance fittings that maintain the integrity of your HPLC systems up to 15,000 psi with mere finger tightening!The use of HPLC systems to achieve faster analyses and increased resolution pushes systems toward higher operating pressures. Our selection of Supel™-Connect High Performance Interconnects and Fittings will assist the chromatographer in maximizing system performance and reliab…
Supelco’s complete line of stock and custom packed GC columns are configured to fit most commercially available GC instruments.Supelco® has been the leader in packed GC column technology for over 40 years. Should you not be able to locate a stock item to fit your needs, our custom capabilities allow us to manufacture columns and packings to your specifications. In addition we also carry hard-to-find tools specifically designed…
High Capacity Gas Purifiers (Remove Moisture and Oxygen)The best purifier choice for removing moisture and oxygen from carrier gas streams is our High Capacity Gas Purifier. It consists of three parts:• Clam-shell oven• Replaceable heating elements• Replaceable converter tube.A convenient starter kit contains all three items for new installations.
Supelcarb® is Back by Popular Demand!Supelco® is pleased to welcome the Supelcarb HC Hydrocarbon trap back to our line of in-line gas purifiers! Supelcarb adsorbent has the greatest trapping ability of hydrocarbons per gram of adsorbent (twice that of activated charcoal). These traps are the best traps available for removing hydrocarbons and other organics from carrier, fuel, air and other gas streams.
Specialty In-Line Purifier for GC-MS HeliumThe most sensitive GC-MS instruments require a steady stream of ultra-high purity (99.99999%) helium for optimal performance. To achieve this level, a specialty purifier is required. These purifiers contain multiple adsorbent beds for the removal of all critical contaminants. Additionally, the adsorbent materials are packed into the cartridge under helium to ensure no other gas off-g…
HPLC and FPLC Columns for the Analysis and Purification of Biopolymers.Biopolymers, including peptides, proteins, polynucleotides, and other biodegradable polymers, display a variety of ionic charges and differ in terms of hydrophobicity, size, shape and mass. In addition to these structural (and functional) complexities, an individual biopolymer is typically present at low concentration in samples that contain many similar co…
Cyclodextrin-based DEX and Astec CHIRALDEX phases are stable, high boiling liquids and make effective CSPs for enantiomer separations by GC. The two lines exhibit complementary selectivity.Cyclodextrins are macromolecules composed of 6 or more D(+)-glucose residues bonded through α-glycosidic linkages. They are classified according to the number of glucose residues they contain: α-cyclodextrins (six residues), β-cyclodextrins…
Active Sampling Tubes for Air Monitoring.ORBO sorbent tubes contain two beds of the same selective adsorbent seperated by glass wool or foam, for gas and vapor sampling. The dual-layer or two-bed construction of the tube allows for any sample breakthough to be captured in the smaller back-up bed. Our sorbent tubes contain Supelco′s high quality adsorbents that professionals world-wide trust for their applications. We offer the…
Supelco′s new Low Adsorption (LA) vials are manufactured using a process that decreases the number of hydroxyl groups on the vial′s glass surface, significantly reducing surface activity while improving analytical quantitation and minimizing pH shifts in the sample.This same process also removes unwanted surface metals such as sodium and boron that can contaminate samples and interfere with trace analysis. Unlike other methods…
Our new certified vial, cap and septa products eliminate "fit" and septa contamination concerns associated with other brands.By taking these extra manufacturing and testing steps, we can ensure:• Caps thread properly onto vials, providing an air-tight seal• Syringe needles are not damaged by irregular vial bottom thickness• Minimal contamination from septa impurities.Quality is built into each component of the Supelco certifie…
The pentafluorophenylpropyl (PFP) stationary phase of Ascentis® Express F5 provides a stable, reversed-phase packing with electron-deficient phenyl rings due to the presence of electronegative fluorines. In addition to forming p-p and mildly steric interactions, F5 phases also retain compounds by polar interactions. As a result of having both polar and non-polar character, F5 phases can show dual-mode retention behavior, some…
This column allows highly reproducible analyses of fatty acid methyl esters (FAMEs), specifically the omega 3 and omega 6 fatty acids. It is tested to ensure reproducible FAME equivalent chain length (ECL) values and resolution of key components. Column Details: Phase: Bonded; poly(ethylene glycol) USP Code: G16 Length: 15, 30 m ID: 0.10, 0.25, 0.32, 0.53 mm df: 0.10, 0.25, 0.50
Ascentis Express HPLC columns, through the use of Fused-Core® particle technology, can provide you with both the high speed and high efficiencies of sub-2 μm particles while maintaining lower backpressures. The combination of high efficiency and low backpressure benefits UPLC® (or other ultra high pressure system) users, as well as conventional HPLC users. Column Details: Mode of chromatography: Hydrophilic interaction…
Application: The 35% phenyl equivalent phase provides a higher polarity option compared to columns containing a lower phenyl content, resulting in a greater retention of polar analytes relative to non-polar compounds. Its selectivity is complementary when paired with SLB-5ms for applications that require dual-column confirmatory analysis, such as for environmental analytes (such as pesticides, PCBs, and herbicides). The low…
The Ascentis Express biphenyl phase chemistry offers alternative selectivity for pharmaceutical analytes and drug metabolites that are not well retained or difficult to resolve on traditional alkyl (C18) and phenyl bonded phases. Ascentis Express HPLC columns, through the use of Fused-Core® particle technology, can provide you with both the high speed and high efficiencies of sub-2 ?m particles while maintaining lower backp…
Tedlar® gas sampling bags are recommended in many US EPA methods including TCLP and methods TO-3 (VOCs), TO-12 (NMOC), TO-14A (VOCs), TO-15 (VOCs), ASTM D-5504 (reduced sulfur compounds) and a variety of atmospheric gas methods. Tedlar® bags are an excellent value and offer several features over competitor versions. Benefits: Unique valve and seam-sealing process ensure bags are sturdy and leak-proof under the mo…
The polar organic and the polar ionic modes have become increasingly popular largely because of their ideal compatibility with MS detection and preparative LC. Two years of extensive research at Astec in understanding these mechanisms has resulted in new possibilities for extending their effectiveness even further. Important changes in linkage chemistries and the silica and the silica have now led to the new CHIROBIOTIC V2 and…
